STARCH GLUE VISCOSITY

How optimal viscosity affects starch glue performance and cardboard quality.

Starch glue context

An extremely large and well-known class of adhesives is based on starch. These play a very large part in industrial production, especially in the packaging industry.

With more and more deliveries being made, the need for cardboard is exploding, being a 71.9 billion dollars market in 2024 and expected to reach 98 billion in 2029.  

With more and more demand, as well as a request from customers for improved quality, the starch glue market is blooming and is in need of always better processes.

Industrial application of starch glue

Starch is principally used for bonding paper products thanks to being a versatile adhesive. Starch based adhesives are used to bond two boxboards, sandwiching a corrugated boxboard for making cartons.

Starch adhesives are readily available, low in cost, and easy to apply from water dispersion. They are considered to be the least expensive class of paper packaging adhesive.

These adhesives are typically supplied to the end-user in powder form and are mixed with water before use to create a relatively thick paste. Formulated starch adhesives can be applied either hot or cold and cure through moisture loss.

Caracteristics of the starch glue making process

Because they form a thermosetting structure when cured, they offer excellent heat resistance. Other notable benefits include their slow curing rate, which allows ample assembly time, and the fact that they are non-toxic and biodegradable. However, they do have drawbacks, such as poor moisture resistance and susceptibility to mold growth.

Importance of the adhesives viscosity

In the production of corrugated cardboard, a wavy structure is used to prepare and assemble the papers and glue. Maintaining control over the adhesive’s viscosity during preparation and application is essential for at the end of the batch, you know your starch glue is okay to be applied

For the production of corrugated cardboard, glue application systems must ensure precise centering of the adhesive on top of the groove and accurately match the quantity of adhesive needed for each type of board. Additionally, the viscosity of the adhesive is crucial.

Impact on cardboard quality

When the viscosity is too low, it leads to imperfections in how the adhesive is removed from the tops of the splines. The meniscus formed during separation can stretch, causing projections or burrs on the sides of the splines, which hinder optimal performance of the inverter. In practice, a viscosity is sought that allows the adhesive to flow smoothly through the application system without causing these defects. The adhesive should distribute evenly over the tops of the splines without creating smudges or projections, even at high speeds.

Rheological complexity of starch glue

The rheological behavior of starch-based adhesives is complex. They are primarily pseudoplastic and thixotropic, and the non-Newtonian properties can vary significantly between products. Therefore, it is essential to control the conditions under which viscosity is measured.

How to install a Sofraser viscometer

MIVI viscometers are versatile measurement instruments and can be placed at different locations on the process.

Installation of a MIVI viscometer in the glue kitchen

The viscosity tool can be placed directly on the glue kitchen tank (A) or on the circulation loop (B) to monitor the batch while cooking and make sure that, at the end of the batch, the starch glue has passed the standard quality required for the cardboard.

Different installation of a MIVI viscometer on the process

Installation of a MIVI viscometer on the process line

You can also install the MIVI viscometer on the process line (C) for a continuous measurement of the viscosity of the starch glue batch as it gets ready to be applied on the cardboard. This installation allows MIVI users to monitor their process in real time.

Why use a Sofraser MIVI viscometer

Thanks to its flexibility, the installation of a MIVI sensor on the production line, in the storage tank or on the starch glue kitchen provides continuous viscosity monitoring to ensure perfect laying of the adhesive. The MIVI viscometer and associated electronics guarantee zero default in glue deposit. This sensor is repeatable and reliable for permanent efficiency.

Key product characteristics:

· Repeatable and reliable for permanent efficiency                                                           

· Easy to install with a wide variety of mountings and positions                                    

· Easy to use

· No drift of measurement in time

· No maintenance

The many customers of the MIVI viscometer in this application are really content with the results they get from their viscosity measurements, which better and ease their process.

Viscosity monitoring and control in the copper wire coating process

The global market for insulating coatings has been booming in recent years. Beside of energy that is the main sector concerned, the electrical, electronics and automotive industries are also key players.

Strict government regulations are being imposed on the market, particularly in North America and Europe. This is forcing coatings manufacturers to go green and adopt sustainable development as part of their program. They are investing in research and development to develop new, innovative products that can be offered at low cost, while complying with regulatory guidelines.

Copper and aluminum wires for electric motors, generators and a wide range of other applications are dip-coated with a very fine, electrically insulating enamel.

The wire coating process is essential for the following main reasons:

  • Provides electrical insulation
    • Protects windings against moisture absorption and heat
    • Improves resistance against shock, vibration and mechanical stress

The most common polymer coatings are formal polyvinyl, polyurethane (PUR) and polyester, which behave differently in terms of adhesion, flexibility, thermal shock and softness.

Coated wires are manufactured by applying a coating of enamel in several layers to a copper conductor filament. The conductor is passed through a bath of liquid enamel or a solution of enamel in a solvent, then heated in an oven to drive off the solvent and harden the enamel.

Why is viscosity monitoring and control essential in the copper plating process?

The general and important factors that make viscosity management important in the copper wire coating process are as follows:

  • Correct properties: Poor coating quality can affect the properties of magnet wires, notably their dielectric strength, flexibility and mechanical properties. Viscosity control helps to warrant constant thickness and uniformity of the coating.
  • Coating quality: Wires must comply with the specifications and regulatory requirements of the finished product, to ensure conformity.
  • Reduce coating errors: Viscosity control can help reduce the frequency of roughening, blistering, bridging and surface erosion errors.
  • Better yield: Ensuring consistency throughout the coating process significantly reduces rejection rates, while cutting costs and time.
  • Cost management: Poor viscosity management increases the use of coating polymer and solvent, which in turn affects companies’ material purchasing costs.
  • Waste: Materials rejected due to poor quality can be reduced through good viscosity management.
  • Efficiency: Eliminating manual viscosity control frees up engineers’ time to concentrate on other tasks.
  • Eco-friendly: Reducing coating polymer and solvent use is good for the environment.

Challenge

Conventional methods of controlling enamel coating viscosity such as flow cups have proved inadequate even in applications where significant variation in enamel viscosity is permitted, and where wire coatings may vary outside the predetermined specification range.

The coating fluid collected during sampling is timed using the dosing cup, the time taken for the liquid to pass through the funnel being taken as an indicator of viscosity. The procedure is tedious and time-consuming, especially if the coating has to be filtered beforehand.

It’s pretty imprecise, inconsistent and unrepeatable even with an experienced operator.

Measurement with the cup is not a real-time or continuous measurement. It cannot detect rapid variations in viscosity.

In order to achieve a high-quality, uniform coating, viscosity change is the key factor to be monitored with continuous and real-time measurement revelations.

Sofraser’s viscometers solutions

MIVI viscosity sensor has been designed and is used to measure the viscosity of all types of liquids and viscous fluids 24/7, providing continuous and instantaneous information. It’s the instrument that ensures everything runs smoothly during the manufacturing and preparation process. What’s more, batch recording ensures perfect traceability.

MIVI viscosity sensor can be matched with one of Sofraser’s electronics that offers a wide range of features from basic on Din rail transmitter to HMI processor with PID control loop.

MIVI process viscometer saves samples and laboratory measurements that are costly and have a long response time that increases the global batch duration. This reduces batching time, resulting in more production. It also helps to determine unexpected events during the whole batch process, enabling you to have complete traceability of the production

Designed to determine viscosity at high shear rate, MIVI comes in different configurations. Ranging from the “Basic” version to the “Sanitary” version including the “Hygienic” version with its design certified by EHEDG.

This viscometer guarantees the irreproachable quality of your final product while respecting the cleanability requirements and thus meeting the latest European standards.

Sofraser’s 50 years of expertise and great track record of decade-lasting sensors allows our clients from all around the world to closely monitor and improve their processes without worry.

The benefits of phenolic resin for wood

Today, many wood manufacturers supply their own plywood mills, producing tons of resin every year. Once produced, the resins are usually stored in huge tanks for a few days, then transported to the sites responsible for putting the material into product. There, the resins are used to impregnate various types of paper, cardboard, plywood and others. These paper products are destined for various markets, such as building materials, as well as for chemical and even aeronautical projects.

Viscosity and phenolic resin

Phenolic resins are specifically produced for paper sizing and impregnation applications. They are distinguished by their ideal characteristics, including outstanding strength and toughness, which make them particularly suitable for these uses. However, the production of phenolic resins is complex and presents considerable challenges due to the demanding reaction conditions required to obtain the final product. These rigorous conditions require precise control and in-depth technical expertise to guarantee the quality and performance of phenolic resins.

And its constraints…

This is because the various ingredients used in phenolic resin production come from different suppliers, and batches are never exactly the same. Each batch is first weighed before being mixed, then heated in a reactor to begin the production cycle.    

Viscosity measurement plays a very important role in: 

  • Polymerization control
  • Indirect moleculor weight monitoring
  • Determination of the reaction end-point for optimal product specification

Moreover, the heating process involves clearly defined steps, with highly sensitive temperature and viscosity values that must be strictly adhered to. As the reaction process for this resin is exothermic, the contents of the reactor can continue to heat up even if the heating process is stopped. As the rate of reaction increases with temperature, there is a risk of the polymerization running out of control and the hardening of the reactor content. Thanks to its high sensitivity, the MIVI will detect this unexpected event at an early stage, enabling the operator to take appropriate action to avoid this manufacturing accident.

Sofraser viscometers for process control

The optimum solution to this problem is the MIVI viscometer. Its installation is safe and reliable, and reaction control becomes more precise thanks to temperature correlation. This device avoids the stresses associated with resin curing, a problem now solved by Sofraser technology. In addition, production stability and quality are improved, and production efficiency is considerably enhanced. Interruptions due to resin curing are eliminated, reducing production and sales losses.

Process viscometer industry

Sofraser is committed to improving your process with this solution. Our experienced team is ready to answer all your questions about the instrument, its installation and after-sales service.

Ink Viscosity for flexographic printing

What is flexographic printing?

Flexography is a commonly used form of printing process which utilizes a flexible relief plate. It can be used for printing on almost any type of substrate, including plastic, metallic films, cellophane, and paper.

Ink Viscosity for flexographic printing

This printing is usually utilised by the food industry on the non-porous substrates required for various types of food packaging; (it is also well suited for printing large areas of solid colour).

The basic principle of each printing technique is the same. To deliver the ink skilfully onto the substrate while ensuring the correct properties according to the process requirements.

The printing market is facing a rapid growth driven primarily by packaging and labels, as online delivery is more and more used.

Crucial ink viscosity

In the pressroom, ink viscosity is critical.

Measuring viscosity is extremely important because knowing the speed and fluidity of the ink helps you know how the ink will perform on the press. But also how fast the press will operate when using a particular ink.

In virtually all printing applications, correct ink viscosity is key to a good ink quality. Ink viscosity characterizes many aspects of how the ink will transfer to its substrate. Its properties can have several effects on absorption, colour strength and drying.

Crucial ink viscosity

Highly viscous inks create stickiness and make it difficult to transfer the image to the substrate, while low viscosity makes the ink more mobile and harder to control, resulting in loss of sharpness and a dirty print.

The strong link between temperature and viscosity means that temperature variations have a significant impact on ink quality. It is therefore important to measure both simultaneously if they evolve together. 

Real-time in-line viscosity control and monitoring in the printing process is essential to improve performance and reduce costs in flexographic printing process.

Sofraser’s expertise on ink viscosity

The installation of a MIVI on tank or a SOFINK on-line viscometer, either on tank, either on the circulation loop, allows you a precise and continuous follow-up of the ink viscosity, to always have the best possible batch.

MIVI process viscometer
MIVI Viscometer

Sofraser’s allows you close monitoring of the ink’s viscosity and temperature in real time and ensures quality in the printing process.

As it is maintenance-free, the sensor doesn’t not to be clean. Its sensitivity in low and high viscosities is also an advantage in this application.

Sofink Viscometer
SOFINK Viscometer

The implementation of a SOFRASER viscometer on your process also allows an overall ink consumption saving of 5%, generating a fast ROI (return on investment).

Using an in-line viscosity sensor to measure and control ink viscosity ensures consistency, consistency and uniformity of ink deposition. All while maximizing printing speed.

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Viscosity of adhesives & sealants

The adhesives & sealants industry

The industry for adhesives and sealants is challenged by the limited raw materials and the negative impact of synthetic compounds on human health and the environment, which an answer is already brought up about: a new generation of adhesives and sealants are now water based, making them less toxic and more environmentally friendly.

Furthermore those products are widely used to assemble, protect and seal systems in construction, manufacture and perform maintenance. They are key components for a lot of projects, therefore their impact is great in the industry itself.

The main raw materials used in the manufacturing of adhesives still come from crude oil and petrochemicals, product whose prices are extremely volatiles and higher than ever.

To ensure a consistent, high-quality and defect-free application of adhesives and sealants, viscosity changes throughout the process flow have to be monitored in real time. Taking measurements from a baseline rather than simply measuring absolute values, and adjusting viscosity by adjusting mix components and temperature compensation helps keeping the process within its specified limits.

Most adhesives are non-Newtonians and viscosity control is prioritized at the end-point, although viscometers can monitor its entirety.

By continuously monitoring viscosity online, preparation and delivery can be controlled more efficiently. Thus significantly improving the flow properties of the final product.

Sofraser’s viscometers

To monitor viscosity throughout the process, the best solution is to install a Sofraser viscometer. More precisely a MIVI sensor with a 9720 multi-product HMI processor, because often, several sealants are produced in the same tank.

mivi sensor viscometer

Compatible across a wide viscosity range, the MIVI can measure from thick pastes to light fluids. Requiring no special preparation, MIVI can be used directly in your process lines. Its ease of use and configuration will allow your operators to use it quickly, easily and with optimal efficiency.

Thanks to their vibrating needle, Sofraser viscometers have a self-cleaning effect, resulting in an almost maintenance free viscosity instrumentation.

Resulting in peak production, the sensor delivers 24/7 instant measurement and is compatible easy to install.

Inventor of the vibrating type technology and with more than 50 years of expertise, Sofraser viscometers are the most reliable process viscometers on the market.

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Viscosity in starch glue manufacturing

Usage of starch glue

Starch glue is principally used for bonding paper products. Most corrugated boxboard for making cartons is bonded with starch based adhesives; starch adhesives are readily available, low in cost, and easy to apply from water dispersion.

Since these adhesives cure to a thermosetting structure, they have excellent heat resistance. Other significant advantages are their very slow curing rate allowing ample assembly time and that they are non-toxic and biodegradable.

The control of the adhesives viscosity at the end of the preparation and during application is critical.

Paper application

Challenges faced by the industry

For the production of corrugated cardboard, glue application systems must allow a perfect centring of the adhesive deposited on top of the groove and fit accurately the quantities of adhesives necessary and sufficient for each type of board manufactured.

Furthermore the viscosity of the adhesive is critical. When the viscosity is too low, this results in imperfections and can cause projections and/or burrs.

In addition, the rheological behaviour of the starch glues is complex. It is mainly pseudo plastic and thixotropic and the non-Newtonian behaviour can be quantitatively significantly different between the two products. This requires to master the conditions of viscosity measurement.

Sofraser’s solution for starch glue viscosity control 

Thanks to its flexibility, the installation of a MIVI sensor on the production line or in storage tank or on starch glue kitchen provides continuous and stable viscosity values during the laying of the adhesive. The MIVI viscometer and associated electronics guarantee zero default in viscosity deposit. This sensor is repeatable and reliable for permanent efficiency.

It is an easy to use and to install solution with a wide variety of mountings and positions available. The plus? No maintenance required.

MIVI viscometer

Coating process and its viscosity for Lithium batteries

The use of lithium batteries

Lithium batteries are safe and reliable and have a wide range of applications including powering electric vehicles. The battery manufacturing process needs to be controlled and optimized in order to guarantee the quality and reliability of the product. Among the global manufacturing process, there is the electrode manufacturing step that includes a coating process. The viscosity of the components and the slurry during the coating process is particularly important. It influences the final quality, efficiency and consistency of the electrode.

A necessary control of viscosity

The viscosity of the polymer binder solution affects the performance of the coating and the ease with which powders are dispersed, as well as the power required for mixing and the speed of application for a uniform coating.

Lithium battery
EV (electric vehicle) Li-Ion battery concept. Close up view. 3d rendering.

Density and viscosity control to optimize batch processes ensures consistency, quality and significant cost savings on materials. Control and traceability of the continuous mixing process can be improved through on-line monitoring and density and viscosity measurements. Automation, supported by on-line integration enables the optimization of all processes on production lines. Battery manufacturing is also speed up to meet growing demand.

A high viscosity of the battery suspension decreases the sedimentation speed at rest and delivers a thicker electrode film at the end of the coating step/phase. But too high viscosity may also make the coating process more difficult to control, which can lead to irregular coating and variable layer density. It resultes in variable ion transfer rates and thus unpredictable battery life (and unpredictable charging cycle time).

Finding the perfect viscosity can be tricky and difficult. The solution is to monitor and controll within the appropriate ranges according to the requirements of the process. With the control of viscosity, batteries and their components are safer and more durable.

The use of viscosimeters

Viscometers are an essential part of the solution for reliable batteries.
Electrodes density has an effect on cycle performance and irreversible loss of capacity in lithium-ion batteries.

The rheological behavior of the slurry is a highly complex one, even within the non-Newtonian fluids. Finding the right balance for an easy to apply product can be very difficult.

MIVI process viscometers provides a high sensitivity viscosity measure that will detect the smallest changes in slurry composition. When combined with the density feature it adds the indirect monitoring of the concentration. Thanks to its instantaneous and continuous measure, combined with the outputs that deliver the measures to the end-user DCS. Sofraser viscometers are a great solution for automated process control, as they are maintenance free and highly reliable.

Similar processes are also valid for solid-state batteries. They are an interesting furure alternative that are a great way to support the growing demand for electric batteries.

Lithium batteries
Lithium batteries

Electric board coating process

Viscosity measurement in electronic board coating process

Dosing the solvent of a coating solution into electronic boards requires precise adjustment. In order to obtain uniform application of the coating; reflected by a constant viscosity. An inhomogeneous coating, either too thick or too thin, can be the source of serious problems. A company’s reputation is at stake if too many customer complaints are related to the poor quality of the finished product. Consequently, costs increase due to inefficient production and raw material losses.

In this way, the installation of a MIVI process viscometer in the circulation loop of the coating process allows the right amount of solvent to be injected into the base resin at the right time during the entire production process.

The MIVI viscometer works continuously, instantly detecting and correcting any viscosity variation.

Use of the MIVI viscometer
Viscosity measurement in electronic board coating process

The printed circuit boards are immersed in a resin-based coating that solidifies at room temperature. The uniformity of the coating reaches 100% quality thanks to the inline viscosity measurement; which also allows a reduction of resin and solvent consumption. Our MIVI inline viscometer allows the achievement of a constant coating viscosity. It increases process repeatability, coating homogeneity and uniformity, and generates material and time savings.

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On-line viscosity measurement in ink deposition on special films

On-line viscosity measurement is the most reliable way to monitor the uniformity and quality of ink deposit on papers; films and specialty substrates. If the process does not allow for consistent ink viscosity, poor batches will be produced. Resulting not only in increased manufacturing costs but also in quality and corporate reputation problems.

The installation of a MIVI on-line viscometer in the ink tank allows a precise and continuous follow-up of the ink viscosity. MIVI adjusts the viscosity of the ink; if necessary according to various parameters such as temperature, flow rate, the need for pigments; solvent addition, chemical reactions and other characteristics related to the production in question.

On-line viscosity measurement in ink deposition on special films
Application of viscosity in printing

The MIVI viscometer ensures permanent operation without time drift and is particle tolerant. It is not necessary to clean the sensor separately from the process. Its sensitivity in low and high viscosities is also an advantage in this application.

As a general rule, the implementation of a MIVI viscometer on press allows an overall ink consumption saving of 5%, generating a return on investment of about one year. The use of an in-line MIVI viscometer ensures the consistency, homogeneity and uniformity of the ink deposit by maximizing the printing speed. MIVI improves print quality, ensuring, among other things, color continuity.

Discover the detailed sheet in English on the use of the MIVI viscometer in printing and coating processes.

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